META TAGS:-RGPV B.PHARMACY 6TH SEM SYLLABUS I RGPV B.PHARMACY 6TH SEM PHARMACEUTICAL ANALYSIS-II SYLLABUS I DOWNLOAD B.PHARMACY 6TH SEM PAPERS I RGPV B.PHARMACY PY-602 SYLLABUS I PHARMACEUTICAL ANALYSIS SYLLABUS I B.PHARMACY COMPLETE SYLLABUS I RGTU B.PHARMACY 6TH SEM SYLLABUS I RGPV B.PHARMA SYLLABUS I B.PHARMACY 6TH SEM RGPV SYLLABUS I DOWNLOAD RGPV B.PHARMACY 6TH SEM PHARMACEUTICAL ANALYSIS PAPERS I PHARMACEUTICAL ANALYSIS-II PAPERS I B.PHARMACY 6TH SEM COMPLETE SYLLABUS DOWNLOAD
The theoretical aspects, basic instrumentation, elements of interpretation of spectra and pharmaceutical application of the following analytical techniques –
- Chromatography: Paper Chromatography TLC, GLC, HPTLC and HPLC.
- Ultraviolet and visible spectrophotometry: Beer-lambart law, electronic transitions, instrumentation, methods, chemical derivatisation, structural analysis,applications.
- Infra red spectrophotometry & FT-IR: Introduction, Theory, instrumentation,interpretation of spectra, its advantages and applications in structure elucidation.
- Fluorimetry.
- Mass Spectroscopy: Introduction, ionization techniques, mass analyzers,fragmentation rules, instrumentation, the mass spectrum & its applications.
- NMR Spectroscopy: Introduction, continuous-wave (CW) NMR spectrometry, pulsed fourier transform spectrometry,chemical shift, pin coupling,spin decoupling & its applications.
- Atomic Absorption.
- X- Ray Diffraction.
- Flame Photometry.
- Immunoassay techniques: Enzymes & radioimmunoassay techniques, theory, methods & its applications.
BOOKS RECOMMENDED:
- Svehla, G. Vogel’s Text Book of Micro and Semi Micro Qualitative Inorganic Analysis, Orient Longman, Hyderabad.
- Beckett, A.H. and Stenlake, J.B., Practical Pharmaceutical Chemistry, TheAthlone Press of the University of London.
- Chatten, L.G., Text Book of Pharmaceutical Chemistry, Marcel Dekker, NewYork.
- Connors, K,.A., A Text Book of Pharmaceutical Analysis, Wiley Interscience,New York.
- Higuchi, J. and Hansen E.B., Pharmaceutical Analysis, Interscience Publisher John Willey and Sons, New York, Sydney.
- Silverstein,R.M., Bassier, G.C., and Morril,T.C., Spectrophotometric Identification of Organic Compounds, John Wiley and Sons Inc.
- Willard, Merritt and Settle, Instrumental Methods of Chemical Analysis,CBS Publisher and Distributors, New Delhi.
- Ewing, G.W., Instrumental Methods of Chemical Analysis,.
LIST OF PRACTICALS :
- Determination of solvent cut off value of different solvents.
- Study of effect of various solvents on spectral features of any drug.
- Perform the quantitative spectrophotometric estimation of drug by single point method.
- Perform the quantitative spectrophotometric estimation of drug by calibration curve method.
- Perform the quantitative spectrophotometric estimation of drug by standard absorptivity method.
- Simultaneous quantitative spectrophotometry estimation of two drugs by simultaneous equation method.
- Simultaneous quantitative spectrophotometric estimation of two drugs by dual wavelength method.
- Simultaneous quantitative spectrometric estimation of two drugs by derivative spectroscopy.
- To determine the drug content of given tablet formulation
- Interpretation of given IR spectra.
- Quantitative estimation of alprazolam (Any drug) by RP-HPLC.
- Simultaneous quantitative estimation of torsemide and spironolactone ( Combination of two drugs) by RP-HPLC.
- Acid and alkaline stress degradation study of any drug.
- Photo and thermal stress degradation study of any drug.
- Oxidative stress degradation study of any drug.
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